4Q79
Structure of a HG-derivative CsgG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-03-13 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.006 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 171.640, 176.880, 104.990 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.247 - 3.100 |
R-factor | 0.2381 |
Rwork | 0.236 |
R-free | 0.27830 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.207 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 |
High resolution limit [Å] | 3.100 | 3.100 |
Number of reflections | 66194 | |
Completeness [%] | 60.0 | 59.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 50mM Tris-HCl (pH 8.5), 300mM MgCl2, 14% PEG2000, VAPOR DIFFUSION, HANGING DROP, temperature 293K |