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4POH

Crystal structure of human Retinoid X Receptor alpha-ligand binding domain complex with 8-methyl UAB30 and the coactivator peptide GRIP-1

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsOTHER
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2004-10-27
DetectorRIGAKU RAXIS IV
Wavelength(s)1.5418
Spacegroup nameP 43 21 2
Unit cell lengths66.250, 66.250, 110.670
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution25.531 - 2.300
R-factor0.2164
Rwork0.216
R-free0.26500
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3oap
RMSD bond length0.008
RMSD bond angle1.100
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.380
High resolution limit [Å]2.3002.300
Rmerge0.0420.259
Number of reflections60097
<I/σ(I)>19.96.8
Completeness [%]99.595.8
Redundancy5.34.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP72954-12% PEG4000, 3-12% Glycerol, 0.1M Bis-Tris, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K

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