4PJZ

CRYSTAL STRUCTURE OF T4 LYSOZYME-GSS-PEPTIDE IN COMPLEX WITH TEICOPLANIN-A2-2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-E
Synchrotron site	APS
Beamline	24-ID-E
Temperature [K]	100
Detector technology	CCD
Collection date	2013-11-22
Detector	ADSC QUANTUM 315
Wavelength(s)	0.97918
Spacegroup name	I 2 2 2
Unit cell lengths	58.116, 63.569, 138.884
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	69.440 - 1.870
R-factor	0.19555
Rwork	0.194
R-free	0.22842
RMSD bond length	0.012
RMSD bond angle	1.577
Refinement software	REFMAC (5.8.0069)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	69.440	1.910
High resolution limit [Å]	1.870	1.880
Rmerge	0.099	0.855
Number of reflections	20297
<I/σ(I)>	15.7	1.79
Completeness [%]	98.9	99.2
Redundancy	5.1	4.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.4	293	19% PEG 3350 ,0.2 M sodium potassium phosphate