4P0I
Structure of the PBP NocT
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2010-10-08 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.987 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 118.860, 69.710, 74.380 |
| Unit cell angles | 90.00, 117.86, 90.00 |
Refinement procedure
| Resolution | 32.430 - 1.890 |
| R-factor | 0.2065 |
| Rwork | 0.205 |
| R-free | 0.23650 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.060 |
| Refinement software | BUSTER (2.10.0) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 38.800 |
| High resolution limit [Å] | 1.890 |
| Number of reflections | 43103 |
| <I/σ(I)> | 22.43 |
| Completeness [%] | 99.4 |
| Redundancy | 6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | 2M SA, 0.1 M Na citrate pH 5.6, 0.2M K tartrate, 5% PEG400 |
