4OZN
GlnK2 from Haloferax mediterranei complexed with ATP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-2 |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-05-08 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 0.8726 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 110.717, 110.717, 76.949 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 44.980 - 2.600 |
| R-factor | 0.21804 |
| Rwork | 0.217 |
| R-free | 0.24348 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.139 |
| Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 47.900 |
| High resolution limit [Å] | 1.440 |
| Number of reflections | 17092 |
| <I/σ(I)> | 8.2 |
| Completeness [%] | 100.0 |
| Redundancy | 5.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 294 | 0.5 M Lithium sulphate, 15% PEG 8000 |
