4OYF
Crystal structure of GLTPH R397A IN Sodium-bound state
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X29A |
| Synchrotron site | NSLS |
| Beamline | X29A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-06-13 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9700 |
| Spacegroup name | P 31 |
| Unit cell lengths | 110.579, 110.579, 306.923 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 12.000 - 3.410 |
| R-factor | 0.28474 |
| Rwork | 0.284 |
| R-free | 0.29348 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.468 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 12.000 |
| High resolution limit [Å] | 3.410 |
| Number of reflections | 48366 |
| <I/σ(I)> | 13.8 |
| Completeness [%] | 87.3 |
| Redundancy | 11.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277 | PEG400 sodium chloride citrate/tris |
