4OWI

peptide structure

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	100
Detector technology	CCD
Collection date	2013-03-01
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.97935
Spacegroup name	P 1 21 1
Unit cell lengths	30.480, 29.390, 32.700
Unit cell angles	90.00, 98.25, 90.00

Refinement procedure

Resolution	30.165 - 1.202
R-factor	0.1632
Rwork	0.162
R-free	0.19470
RMSD bond length	0.011
RMSD bond angle	1.157
Refinement software	PHENIX ((phenix.refine: 1.7.1_743))

Data quality characteristics

	Overall
Low resolution limit [Å]	30.165
High resolution limit [Å]	1.200
Number of reflections	17562
<I/σ(I)>	59.73
Completeness [%]	97.5
Redundancy	6.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		291.15	ethanol