4NAQ
Crystal structure of porcine aminopeptidase-N complexed with poly-alanine
Replaces: 4HOLReplaces: 4FKFExperimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 4.2.2 |
| Synchrotron site | ALS |
| Beamline | 4.2.2 |
| Detector technology | CCD |
| Detector | NOIR-1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 260.160, 62.744, 81.490 |
| Unit cell angles | 90.00, 100.28, 90.00 |
Refinement procedure
| Resolution | 50.000 - 2.100 |
| R-factor | 0.1478 |
| Rwork | 0.145 |
| R-free | 0.19812 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.278 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.100 |
| Number of reflections | 71538 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
