4N9R

X-ray structure of the complex between hen egg white lysozyme and pentacholrocarbonyliridate(III) (1 day)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Wavelength(s)	1.5418
Spacegroup name	P 43 21 2
Unit cell lengths	78.319, 78.319, 37.049
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	25.450 - 1.550
R-factor	0.184
Rwork	0.157
R-free	0.19420
Structure solution method	FOURIER SYNTHESIS
Starting model (for MR)	193l
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.500
Number of reflections	34873
Completeness [%]	98.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.5		Crystals of the complex have been obtained by soaking pre-grown HEWL crystals in a satured solution of Ir(Cl)5CO for 1 day, pH 4.5, VAPOR DIFFUSION, HANGING DROP