4MXI
ClpP Ser98dhA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-03-16 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 121.590, 121.590, 402.950 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 15.000 - 2.300 |
| R-factor | 0.19741 |
| Rwork | 0.196 |
| R-free | 0.22075 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3v5e |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.890 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.400 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.057 | 0.589 |
| Number of reflections | 79191 | |
| <I/σ(I)> | 23.34 | 4.85 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 9.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4 | 293 | 0.1 M Citric acid, 2.0 M (NH4)2SO4, pH 4.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
