4M3C
Structure of a binary complex between homologous tetrameric legume lectins from Butea monosperma and Spatholobus parviflorus seeds
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2012-02-26 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54179 |
Spacegroup name | P 1 |
Unit cell lengths | 77.110, 78.630, 96.190 |
Unit cell angles | 96.00, 89.99, 100.37 |
Refinement procedure
Resolution | 15.840 - 2.500 |
R-factor | 0.2151 |
Rwork | 0.211 |
R-free | 0.28900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.888 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | Auto (MR) |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.840 | |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 69131 | |
Completeness [%] | 95.0 | 95 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 294 | 25% PEG-8000, 5% MPD, Phosphate buffer, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 294K |