4LKC
An Antibody Against the C-terminal Domain of PCSK9 lowers LDL Cholesterol Levels in vivo
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-01-31 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.0003 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 92.062, 62.338, 84.014 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.570 - 2.200 |
R-factor | 0.1752 |
Rwork | 0.172 |
R-free | 0.24510 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.100 |
Refinement software | BUSTER (2.9.5) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 92.060 |
High resolution limit [Å] | 2.190 |
Number of reflections | 25422 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | 12.6% PEG 3350, 0.01 M spermine tetrahydrochloride, 0.0126 M trisodium citrate, pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |