4LKA
Crystal Structure of MOZ double PHD finger histone H3K9ac complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-06-23 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97372 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 70.455, 70.455, 96.370 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.255 - 1.610 |
R-factor | 0.1652 |
Rwork | 0.164 |
R-free | 0.18520 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4lk9 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.170 |
Data reduction software | XDS |
Data scaling software | SCALA (0.1.27) |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.190 |
High resolution limit [Å] | 1.610 |
Rmerge | 0.076 |
Number of reflections | 32149 |
Completeness [%] | 100.0 |
Redundancy | 11 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 283 | 100 mM Na-Hepes, 1.4 M sodium citrate, pH 7.5, vapor diffusion, temperature 283K |