4LK8
Crystal structure of CyaY protein from Psychromonas ingrahamii in complex with Co(II)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-04-02 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.91907 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 39.891, 50.564, 46.310 |
Unit cell angles | 90.00, 90.77, 90.00 |
Refinement procedure
Resolution | 30.425 - 1.494 |
R-factor | 0.1853 |
Rwork | 0.184 |
R-free | 0.21060 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4hs5 |
RMSD bond length | 0.019 |
RMSD bond angle | 1.781 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.425 | 30.430 | 1.550 |
High resolution limit [Å] | 1.494 | 3.230 | 1.500 |
Number of reflections | 53634 | ||
Completeness [%] | 92.0 | 87.1 | 77.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.8 | 297 | 20mM sodium acetate, 200mM MgCl2, 29.5% PEG 4000, pH 4.8, VAPOR DIFFUSION, HANGING DROP, temperature 297.0K |