4LFP

X-ray structure of the adduct between hen egg white lysozyme and a homoleptic gold(I) complex with the saccharynate ligand

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	ENRAF-NONIUS FR571
Temperature [K]	100
Detector technology	CCD
Collection date	2013-02-11
Detector	RIGAKU SATURN 944
Wavelength(s)	1.5418
Spacegroup name	P 43 21 2
Unit cell lengths	78.046, 78.046, 37.317
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	21.650 - 1.720
R-factor	0.18
Rwork	0.180
R-free	0.23600
Structure solution method	FOURIER SYNTHESIS
Starting model (for MR)	4j1a
RMSD bond length	0.020
RMSD bond angle	2.000
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	21.650
High resolution limit [Å]	1.720
Rmerge	0.075
Number of reflections	12749
Completeness [%]	99.3
Redundancy	6.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1