4LDR

Structure of the S283Y mutant of MRDI

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.2
Synchrotron site	ALS
Beamline	5.0.2
Detector technology	CCD
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.0
Spacegroup name	P 21 21 21
Unit cell lengths	44.518, 115.970, 135.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.053 - 2.292
R-factor	0.1813
Rwork	0.180
R-free	0.20750
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.005
RMSD bond angle	0.958
Refinement software	PHENIX ((phenix.refine: 1.8.2_1309))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	88.107
High resolution limit [Å]	2.292	2.292
Number of reflections	32107

Crystallization Conditions

crystal ID	method	pH	temperature	details
1