Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-6A |
| Synchrotron site | Photon Factory |
| Beamline | BL-6A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-11-07 |
| Detector | ADSC QUANTUM 4r |
| Wavelength(s) | 0.97898, 0.97926, 0.96403 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 43.504, 135.958, 51.568 |
| Unit cell angles | 90.00, 92.51, 90.00 |
Refinement procedure
| Resolution | 41.399 - 2.000 |
| R-factor | 0.1666 |
| Rwork | 0.165 |
| R-free | 0.20530 |
| Structure solution method | MAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.996 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 79331 |
| Completeness [%] | 99.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 0.2M Ammonium sulfate, 0.1M BIS-TRIS pH6.5, 25% w/v PEG 3350, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
