4KTZ
Lactococcus phage 67 RuvC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-10-23 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9796 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 66.710, 66.970, 71.080 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.110 - 1.900 |
R-factor | 0.20451 |
Rwork | 0.202 |
R-free | 0.25374 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ktw |
RMSD bond length | 0.013 |
RMSD bond angle | 1.243 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.800 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 29210 | |
<I/σ(I)> | 8.1 | 2.4 |
Completeness [%] | 94.5 | 88.3 |
Redundancy | 3.3 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 290 | 0.4 M MgCl2, 25% w/v PEG2000, 0.1M HEPES pH7, VAPOR DIFFUSION, HANGING DROP, temperature 290K |