4KRW
Novel re-arrangement of an RsmA/cSRa family protein to create a structurally distinct new RNA-binding family member
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-01-01 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.9334 |
Spacegroup name | P 31 1 2 |
Unit cell lengths | 41.137, 41.137, 72.530 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.630 - 2.010 |
R-factor | 0.2272 |
Rwork | 0.218 |
R-free | 0.31444 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.016 |
RMSD bond angle | 2.126 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER (MR) |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 35.630 |
High resolution limit [Å] | 2.010 |
Completeness [%] | 98.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 292 | 0.2 M sodium iodide, 20% (v/v) PEG 3350, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 292K |