4KMP
Structure of XIAP-BIR3 and inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Detector technology | CCD |
| Collection date | 2010-02-02 |
| Detector | RIGAKU SATURN 944+ |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 |
| Unit cell lengths | 32.016, 33.281, 48.002 |
| Unit cell angles | 77.97, 70.54, 61.28 |
Refinement procedure
| Resolution | 20.250 - 1.950 |
| R-factor | 0.1647 |
| Rwork | 0.162 |
| R-free | 0.21870 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1g73 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.334 |
| Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.250 |
| High resolution limit [Å] | 1.950 |
| Number of reflections | 9907 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.8 | 291 | 0.1M Bis-tri pH5.8, 2M (NH4)2SO4, VAPOR DIFFUSION, HANGING DROP, temperature 291K |
