4KMM

M76H variant of human ferrochelatase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 22-BM
Synchrotron site	APS
Beamline	22-BM
Detector technology	CCD
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	1.0
Spacegroup name	P 21 21 21
Unit cell lengths	88.138, 93.418, 110.219
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	71.260 - 2.600
R-factor	0.20772
Rwork	0.205
R-free	0.25916
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.017
RMSD bond angle	1.870
Refinement software	REFMAC (5.5.0102)

Data quality characteristics

	Overall
Low resolution limit [Å]	71.260
High resolution limit [Å]	2.600
Number of reflections	26185
Completeness [%]	86.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1