4KLD
DNA polymerase beta matched substrate complex with Ca2+, 0 s
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-08-13 |
Detector | RIGAKU SATURN 92 |
Wavelength(s) | 1.54178 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.800, 80.400, 55.500 |
Unit cell angles | 90.00, 107.90, 90.00 |
Refinement procedure
Resolution | 23.147 - 1.916 |
R-factor | 0.2019 |
Rwork | 0.197 |
R-free | 0.25050 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3c2m |
RMSD bond length | 0.011 |
RMSD bond angle | 1.237 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | PHENIX (1.7_650) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.990 |
High resolution limit [Å] | 1.916 | 4.140 | 1.916 |
Rmerge | 0.064 | 0.042 | 0.483 |
Number of reflections | 30191 | ||
<I/σ(I)> | 15.6 | ||
Completeness [%] | 97.7 | 95.1 | 92 |
Redundancy | 4.6 | 5.7 | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 291 | 50 mM imidazole, 350 mM sodium chloride, 17% PEG3350, pH 8.0, VAPOR DIFFUSION, temperature 291K |