4JN5
Crystal structures of the first condensation domain of the CDA synthetase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Detector technology | IMAGE PLATE |
Collection date | 2011-02-14 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 62.130, 82.438, 87.732 |
Unit cell angles | 90.00, 106.34, 90.00 |
Refinement procedure
Resolution | 33.905 - 2.440 |
R-factor | 0.2036 |
Rwork | 0.200 |
R-free | 0.25670 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.497 |
Refinement software | PHENIX ((phenix.refine: 1.7_650)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.440 |
Number of reflections | 31620 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 9-13% PEG 10000, 0.1 M HEPES, VAPOR DIFFUSION, SITTING DROP, temperature 277K |