4J78
Crystal structure of beta'-COP/Emp47p complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 24-ID-E |
| Synchrotron site | APS |
| Beamline | 24-ID-E |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 315 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 75.187, 51.220, 85.137 |
| Unit cell angles | 90.00, 101.60, 90.00 |
Refinement procedure
| Resolution | 36.825 - 1.478 |
| R-factor | 0.1426 |
| Rwork | 0.142 |
| R-free | 0.16280 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.251 |
| Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 83.397 |
| High resolution limit [Å] | 1.478 |
| Number of reflections | 51789 |
| Completeness [%] | 97.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
