4IVG
Crystal structure of mitochondrial Hsp90 (TRAP1) NTD-Middle domain dimer with AMPPNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-09-14 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.115869 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 85.146, 94.509, 155.456 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.546 - 1.749 |
R-factor | 0.1891 |
Rwork | 0.189 |
R-free | 0.20260 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.117 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: dev_1214)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.810 |
High resolution limit [Å] | 1.750 | 1.750 |
Number of reflections | 63000 | |
<I/σ(I)> | 1.44 | |
Completeness [%] | 99.4 | 94.6 |
Redundancy | 7.8 | 6.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1M Sodium Phosphate monobasic monohydrate pH 6.5, 12% PEG 8000, VAPOR DIFFUSION, HANGING DROP, temperature 293K |