4IRH
Auto-inhibited ERG Ets domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2012-08-02 |
Detector | MAR scanner 300 mm plate |
Wavelength(s) | 0.9787 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 44.741, 44.741, 175.083 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.280 - 2.100 |
R-factor | 0.18238 |
Rwork | 0.181 |
R-free | 0.21495 |
Structure solution method | SAD |
RMSD bond length | 0.022 |
RMSD bond angle | 1.752 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.280 | 2.140 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 6372 | |
Completeness [%] | 99.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 290 | 1.4M Sodium Citrate, pH 4.5, VAPOR DIFFUSION, SITTING DROP, temperature 290K |