4HTZ

Crystal structure of PDE2 catalytic domain in space group P1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	CCD
Collection date	2012-06-27
Detector	ADSC QUANTUM 315
Wavelength(s)	0.9793
Spacegroup name	P 1
Unit cell lengths	56.190, 73.870, 92.610
Unit cell angles	109.68, 91.71, 90.91

Refinement procedure

Resolution	33.814 - 2.000
R-factor	0.1915
Rwork	0.188
R-free	0.24880
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.043
Data reduction software	iMOSFLM
Phasing software	MOLREP
Refinement software	PHENIX ((phenix.refine: 1.7.1_743))

Data quality characteristics

	Overall
Low resolution limit [Å]	33.814
High resolution limit [Å]	2.000
Number of reflections	88029

Crystallization Conditions

crystal ID	method	pH	temperature	details
1