4GT9
T. Maritima FDTS with FAD, dUMP and Folate.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-03-11 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.9809 |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 110.320, 110.320, 120.570 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.580 - 1.390 |
R-factor | 0.15295 |
Rwork | 0.152 |
R-free | 0.16416 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1o26 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.756 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.430 |
High resolution limit [Å] | 1.390 | 1.390 |
Rmerge | 0.043 | 0.876 |
Number of reflections | 74209 | |
<I/σ(I)> | 27.7 | 2.7 |
Completeness [%] | 99.6 | 99.9 |
Redundancy | 8.4 | 8.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.58 | 295 | 3-6% PEG 4K (w/v), 200mM NaCl, 100 mM Na/K phosphate (pH 6.58), VAPOR DIFFUSION, HANGING DROP, temperature 295K |