4GOJ
The Crystal Structure of full length Arl3GppNHp in complex with UNC119a
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Detector technology | CCD |
Collection date | 2012-02-29 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 69.750, 103.300, 119.890 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.970 | 2.200 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.098 | 0.395 |
Number of reflections | 51107 | |
<I/σ(I)> | 13.06 | |
Completeness [%] | 99.6 | 99.7 |
Redundancy | 5.53 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 3.4 M Sodium Formate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |