4GM5

Carboxypeptidase T with Sulphamoil Arginine

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL41XU
Synchrotron site	SPring-8
Beamline	BL41XU
Temperature [K]	100
Detector technology	CCD
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	0.8
Spacegroup name	P 63 2 2
Unit cell lengths	158.050, 158.050, 104.980
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	20.000 - 1.390
R-factor	0.14327
Rwork	0.142
R-free	0.16225
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.329
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	REFMAC (5.7.0029)

Data quality characteristics

	Overall
Low resolution limit [Å]	26.950
High resolution limit [Å]	1.388
Rmerge	0.067
Number of reflections	151202
<I/σ(I)>	15.7916
Completeness [%]	99.1
Redundancy	4.97

Crystallization Conditions

crystal ID	method	pH	temperature	details
1