4GI2
Crotonyl-CoA Carboxylase/Reductase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 76 |
Detector technology | PIXEL |
Collection date | 2011-12-08 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.001 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 91.400, 91.400, 206.100 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.182 - 3.000 |
R-factor | 0.185 |
Rwork | 0.182 |
R-free | 0.24080 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3krt 3hzz |
RMSD bond length | 0.009 |
RMSD bond angle | 1.252 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELXD |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.100 |
High resolution limit [Å] | 3.000 | 3.000 |
Number of reflections | 20867 | |
Completeness [%] | 97.2 | 97.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 291 | 4M Sodium formate, pH 8, VAPOR DIFFUSION, SITTING DROP, temperature 291K |