4GCH

STRUCTURE AND ACTIVITY OF TWO PHOTOREVERSIBLE CINNAMATES BOUND TO CHYMOTRYPSIN

Experimental procedure

Spacegroup name	P 42 21 2
Unit cell lengths	69.700, 69.700, 97.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.000 - 1.900
R-factor	0.209
RMSD bond length	0.021
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	1.900 *
Rmerge	0.052 *
Number of reflections	10856 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	other *	5.6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	chymotrypsin	15 (mg/ml)
2	1	1	sodium cacodylate	10 (mM)
3	1	1	cetyltrimethylammonium bromide	0.75 (%sat)
4	1	1	ammonium sulfate	45 (%sat)
5	1	2	ammonium sulfate	65 (%sat)