4FYU
Crystal structure of Thioredoxin from Wuchereria bancrofti at 2.0 Angstrom
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X13 |
Synchrotron site | EMBL/DESY, Hamburg |
Beamline | X13 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.8123 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 112.610, 112.610, 162.050 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.250 - 2.000 |
R-factor | 0.173 |
Rwork | 0.170 |
R-free | 0.21800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.020 |
RMSD bond angle | 2.015 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.940 |
Number of reflections | 35142 |
Completeness [%] | 97.0 |
Redundancy | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 293 | 100mM Tris HCL pH 5.6, 200mM NaCl, 24% PEG 3350, VAPOR DIFFUSION, HANGING DROP, temperature 293K |