4EGZ

Crystal Structure of AraR(DBD) in complex with operator ORR3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE BM14
Synchrotron site	ESRF
Beamline	BM14
Temperature [K]	100
Detector technology	CCD
Collection date	2010-07-01
Detector	MAR CCD 165 mm
Wavelength(s)	1.0
Spacegroup name	P 43
Unit cell lengths	46.160, 46.160, 171.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.629 - 2.300
R-factor	0.2224
Rwork	0.220
R-free	0.27120
Structure solution method	SAD
RMSD bond length	0.010
RMSD bond angle	1.208
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SHELXS
Refinement software	REFMAC (5.5.0072)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.300
Completeness [%]	99.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.2	298	0.1M sodium acetate, 200mM KCl, 25% PEG 8000, pH 4.2, VAPOR DIFFUSION, HANGING DROP, temperature 298K