4EFU
Hsp90 Alpha N-terminal Domain in Complex with an Inhibitor 6-Hydroxy-3-(3-methyl-benzyl)-1H-indazole-5-carboxylic acid benzyl-methyl-amide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Wavelength(s) | 1.54 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 67.588, 90.623, 98.788 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.170 - 2.000 |
R-factor | 0.2051 |
Rwork | 0.204 |
R-free | 0.22310 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.100 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | BUSTER (2.11.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 35.170 |
High resolution limit [Å] | 2.000 |
Number of reflections | 19812 |
Completeness [%] | 94.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | Na-Cacodylate, 30% PEG8000, 0.2M Ammonium Sulfate , pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |