4DZN
A de novo designed Coiled Coil CC-pIL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-10-10 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.7 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 24.723, 40.943, 87.430 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.720 - 1.590 |
R-factor | 0.15714 |
Rwork | 0.155 |
R-free | 0.19844 |
Structure solution method | AB INITIO PHASING+MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.115 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | ACORN |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.720 | 1.700 |
High resolution limit [Å] | 1.590 | 1.600 |
Number of reflections | 11991 | |
Completeness [%] | 96.1 | 95.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 291 | 0.2 M NH4H2PO4, 0.1 M Tris, 50% v/v MPD, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 291K |