4DBA
Designed Armadillo repeat protein (YIIM3AII)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 2010-11-11 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 |
Unit cell lengths | 56.151, 60.603, 61.862 |
Unit cell angles | 74.82, 89.55, 75.53 |
Refinement procedure
Resolution | 25.288 - 2.400 |
R-factor | 0.237 |
Rwork | 0.234 |
R-free | 0.30140 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.203 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 36.560 |
High resolution limit [Å] | 2.400 |
Rmerge | 0.057 |
Number of reflections | 26658 |
<I/σ(I)> | 2.1 |
Completeness [%] | 92.8 |
Redundancy | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4 | 293 | 0.05 M succinic acid, pH 4.0, 20% PEG 4000, 0.2 M Li2SO4, VAPOR DIFFUSION, SITTING DROP, temperature 293K |