4D4O
Crystal Structure of the Kti11 Kti13 heterodimer Spacegroup P64
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
| Synchrotron site | PETRA III, EMBL c/o DESY |
| Beamline | P14 (MX2) |
| Temperature [K] | 100 |
| Collection date | 2013-11-07 |
| Spacegroup name | P 64 |
| Unit cell lengths | 151.270, 151.270, 107.140 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 75.635 - 2.897 |
| R-factor | 0.1991 |
| Rwork | 0.198 |
| R-free | 0.21880 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.627 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.970 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Rmerge | 0.100 | |
| Number of reflections | 30909 | |
| <I/σ(I)> | 20.33 | 1.5 |
| Completeness [%] | 99.4 | 94.1 |
| Redundancy | 11.06 | 10 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 100 MM TRIS PH 7.4, 2 M LI2SO4 |
