4D2P
Structure of MELK in complex with inhibitors
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-07-30 |
Detector | RIGAKU SATURN |
Spacegroup name | P 1 |
Unit cell lengths | 66.284, 76.026, 78.596 |
Unit cell angles | 85.86, 69.87, 90.17 |
Refinement procedure
Resolution | 41.030 - 2.550 |
R-factor | 0.2375 |
Rwork | 0.234 |
R-free | 0.31170 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.011 |
RMSD bond angle | 1.140 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Refinement software | BUSTER (2.11.5) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.000 |
High resolution limit [Å] | 2.550 |
Rmerge | 0.070 |
Number of reflections | 46777 |
<I/σ(I)> | 5.5 |
Completeness [%] | 84.8 |
Redundancy | 1.72 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |