Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-09-23 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 41.480, 83.880, 68.944 |
| Unit cell angles | 90.00, 103.92, 90.00 |
Refinement procedure
| Resolution | 33.460 - 2.200 |
| R-factor | 0.19676 |
| Rwork | 0.194 |
| R-free | 0.23969 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1e25 |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.619 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.940 | 2.320 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Rmerge | 0.140 | 0.650 |
| Number of reflections | 23354 | |
| <I/σ(I)> | 10.5 | 3.1 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 6.8 | 6.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 0.1 M HEPES, 1.5 M SODIUM CITRATE BUFFER (PH 7.5). |
