4CZ0
Structure of the A_mallard_Sweden_51_2002 H10 Avian Haemmaglutinin in complex with avian receptor analog Su-3SLN
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 69.113, 216.085, 81.486 |
| Unit cell angles | 90.00, 105.23, 90.00 |
Refinement procedure
| Resolution | 108.040 - 3.200 |
| R-factor | 0.26604 |
| Rwork | 0.264 |
| R-free | 0.30273 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4cvy |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.850 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.930 | 3.370 |
| High resolution limit [Å] | 3.200 | 3.200 |
| Rmerge | 0.170 | 0.950 |
| Number of reflections | 37572 | |
| <I/σ(I)> | 7.2 | 1.4 |
| Completeness [%] | 98.9 | 99.5 |
| Redundancy | 3.5 | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 18% PEG 2000MME AND 0.1 M BICINE PH 9.0 |
