4CYD
GlxR bound to cAMP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PIXEL |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 63.930, 102.660, 82.220 |
| Unit cell angles | 90.00, 108.49, 90.00 |
Refinement procedure
| Resolution | 29.410 - 1.820 |
| R-factor | 0.19216 |
| Rwork | 0.189 |
| R-free | 0.24553 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.908 |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 29.400 |
| High resolution limit [Å] | 1.820 |
| Rmerge | 0.040 |
| Number of reflections | 88615 |
| <I/σ(I)> | 15.3 |
| Completeness [%] | 98.5 |
| Redundancy | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
