4CUQ
Crystal structure of human BAZ2B in complex with fragment-2 N09594
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-04-30 |
| Detector | DECTRIS PIXEL |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 82.760, 96.500, 57.700 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 17.866 - 2.110 |
| R-factor | 0.1699 |
| Rwork | 0.167 |
| R-free | 0.22570 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.992 |
| Data scaling software | Aimless |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.850 | 2.160 |
| High resolution limit [Å] | 2.110 | 2.110 |
| Rmerge | 0.060 | 0.730 |
| Number of reflections | 13598 | |
| <I/σ(I)> | 18.2 | 2.8 |
| Completeness [%] | 99.5 | 99.2 |
| Redundancy | 5.5 | 5.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.4 | 33% PEG SMEAR LOW, 0.1M MES PH 6.4 |
