4CPP

CRYSTAL STRUCTURES OF CYTOCHROME P450-CAM COMPLEXED WITH CAMPHANE, THIOCAMPHOR, AND ADAMANTANE: FACTORS CONTROLLING P450 SUBSTRATE HYDROXYLATION

Experimental procedure

Spacegroup name	P 21 21 21
格子定数 [Å]	108.670, 103.900, 36.380
格子定数 [度]	90.00, 90.00, 90.00

精密化法

分解能	? - 2.110
R因子	0.184
結合長の平均二乗偏差(RMSD) [Å]	0.019
結合角の平均二乗偏差(RMSD) [度]	0.037 *
Refinement software	PROFFT

Quality characteristics

	Overall
Rmerge_l_obs	0.079 *
Total number of observations	144737 *

文献の結晶化試薬

ID	結晶ID	溶液	試薬名	濃度 (単位) (単位)	詳細
1	1	1	P-450CAM	1 (mM)	camphor free
2	1	1		250 (mM)
3	1	1	dithiothreitol	50 (mM)
4	1	2	ammonium sulfate	66-70 (%sat)	with 5M KOH