4CMY

Chlorobium tepidum Ferritin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	P 21 21 21
Unit cell lengths	123.310, 190.370, 242.070
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	103.710 - 2.590
R-factor	0.19421
Rwork	0.193
R-free	0.21788
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.014
RMSD bond angle	1.601
Refinement software	REFMAC (5.7.0029)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	100.000	2.730
High resolution limit [Å]	2.590	2.590
Rmerge	0.150	0.700
Number of reflections	169035
<I/σ(I)>		2.2
Completeness [%]	100.0	100
Redundancy	6.6	5.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1