4CMV

Crystal structure of Rv3378c

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.3.1
Synchrotron site	ALS
Beamline	8.3.1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	P 21 21 21
Unit cell lengths	57.705, 94.983, 111.161
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.317 - 2.307
R-factor	0.1906
Rwork	0.189
R-free	0.22870
Structure solution method	SAD
Starting model (for MR)	NONE
RMSD bond length	0.009
RMSD bond angle	1.171
Data reduction software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((PHENIX.REFINE: 1.8.2_1309))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.340
High resolution limit [Å]	2.300	2.300
Rmerge	0.120	0.570
Number of reflections	51789
<I/σ(I)>	15.1	2.1
Completeness [%]	100.0	100
Redundancy	4.1	4.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1