4CLN

STRUCTURE OF A RECOMBINANT CALMODULIN FROM DROSOPHILA MELANOGASTER REFINED AT 2.2-ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 1
Unit cell lengths	29.570, 53.920, 24.780
Unit cell angles	93.24, 97.08, 88.86

Refinement procedure

Resolution	10.000 - 2.200
R-factor	0.197
RMSD bond length	0.018
RMSD bond angle	0.043
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000 *
High resolution limit [Å]	2.200 *
Total number of observations	10617 *
Number of reflections	6831 *
Completeness [%]	81.7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	MPD	50 (%(v/v))
2	1	reservior	ethanol	15 (%(v/v))
3	1	reservoir	calcium chloride	5 (mM)
4	1	reservoir	sodium acetate	20 (mM)
5	1	drop	protein	5.3 (mg/ml)