4CKT
PIH1 N-terminal domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-09-30 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 50.020, 62.150, 114.290 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 54.599 - 3.000 |
| R-factor | 0.2267 |
| Rwork | 0.224 |
| R-free | 0.28140 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.838 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | SHELX |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 61.670 | 3.140 |
| High resolution limit [Å] | 3.060 | 3.060 |
| Rmerge | 0.120 | 0.520 |
| Number of reflections | 68364 | |
| <I/σ(I)> | 15.4 | 2.5 |
| Completeness [%] | 90.1 | 56.4 |
| Redundancy | 10.8 | 4.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | pH 7 |
