4CJ0

Crystal structure of CelD in complex with affitin E12

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF
Synchrotron site	ESRF
Beamline	ID23-2
Temperature [K]	100
Spacegroup name	P 43
Unit cell lengths	87.633, 87.633, 97.426
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	43.850 - 1.100
R-factor	0.10773
Rwork	0.107
R-free	0.12546
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1clc
RMSD bond length	0.026
RMSD bond angle	2.030
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.7.0029)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.710	1.120
High resolution limit [Å]	1.100	1.100
Rmerge	0.110	0.750
Number of reflections	292047
<I/σ(I)>	10.5	2.9
Completeness [%]	98.4	96.3
Redundancy	5.8	5.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1