4CJ0
Crystal structure of CelD in complex with affitin E12
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 100 |
| Spacegroup name | P 43 |
| Unit cell lengths | 87.633, 87.633, 97.426 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 43.850 - 1.100 |
| R-factor | 0.10773 |
| Rwork | 0.107 |
| R-free | 0.12546 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1clc |
| RMSD bond length | 0.026 |
| RMSD bond angle | 2.030 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.710 | 1.120 |
| High resolution limit [Å] | 1.100 | 1.100 |
| Rmerge | 0.110 | 0.750 |
| Number of reflections | 292047 | |
| <I/σ(I)> | 10.5 | 2.9 |
| Completeness [%] | 98.4 | 96.3 |
| Redundancy | 5.8 | 5.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
