4CGE

Crystal structure of Mycobacterium tuberculosis Resuscitation promoting factor E

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.3.1
Synchrotron site	ALS
Beamline	8.3.1
Temperature [K]	100
Collection date	2012-07-13
Spacegroup name	P 1 21 1
Unit cell lengths	34.543, 84.004, 72.628
Unit cell angles	90.00, 103.53, 90.00

Refinement procedure

Resolution	42.002 - 2.756
R-factor	0.2364
Rwork	0.234
R-free	0.28990
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.002
RMSD bond angle	0.580
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	42.000
High resolution limit [Å]	2.760
Rmerge	0.130
Number of reflections	10498
Completeness [%]	94.5
Redundancy	3.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1